Practical Manual of Analytical Chemistry
By Neelam Singla, Navneet Kaur and Kanchan Kohli
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Contents:
LIMIT TEST
1. To perform the limit test for chlorides in the given sample of Sodium Chloride (NaCl)
2. To perform the limit test for sulphate in the given sample of Potassium Sulphate (K2SO4)
3. To perform the limit test for iron in the given sample of Sodium Chloride (NaCl)
4. To perform the limit test for arsenic in the given sample of Magnesium Sulphate (MgSO4)
5. To Prepare and standardize 250 ml of approximately 0.1N Sodium Hydroxide (NaOH)
6. To Prepare and standardize 250 ml of approximately 0.1N Sulphuric acid (H2SO4)
7. To Prepare and standardize 250 ml of approximately 0.1M Sodium thiosulphate (Na2S2O3)
8. To prepare and standardize 250 ml of approximately 0.1 N Potassium permanganate (KMNO4)
9. To prepare and standardize 250 ml of approximately 0.1 N Ceric Ammonium Sulphate (NH4Ce (SO4)4) 2H2O
10. To determine the % age purity of given sample of Ammonium Chloride.
11. To find out the percentage purity of given sample of Ferrous Sulphate (FeSO4.7H2O)
12. To determine the percentage purity of given sample of Copper Sulphate (CuSO4.5H2O)
13. To find out the % age purity of given sample of Calcium Gluconate
14. To determine the % age purity of given sample of Hydrogen Peroxide (H2O2).
15. To determine the % age purity of given sample of Sodium
Benzoate
16. To determine the % age purity of given sample of Sodium chloride. ELECTRO ANALYTICAL METHODS
17. To determine the normality of strong acid (H2SO4) in the given unknown solution by titrating against strong base (NaOH) using conductometry.
18. To determine the normality of strong acid (H2SO4) and weak acid (CH3COOH) in the given unknown solution by titrating against strong base (NaOH) using conductometry
19. To determine the normality of strong acid (H2SO4) in the given unknown solution by titrating against strong base (NaOH) potentiometrically.
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Practical Manual of Analytical Chemistry - Neelam Singla
Practical Manual of
Analytical Chemistry
Second Edition
Practical Manual of
Analytical Chemistry
Second Edition
Practical Manual of Analytical Chemistry, Second Edition
by Neelam Singla, Navneet Kaur and Kanchan Kohli
© 2019, by Publisher
All rights reserved. No part of this book or parts thereof may be reproduced, stored in a retrieval system or transmitted in any language or by any means, electronic, mechanical, photocopying, recording or otherwise without the prior written permission of the publishers.
Published by
Printed at
Aditya Offset Process (I) Pvt. Ltd.
Hyderabad.
Price: Rs. 175.00
ISBN: 978-93-89354-06-5 (Paperback)
Preface
It gives us immense pleasure in bringing out the second edition of the book Practical Manual of Analytical Chemistry for Ist year students of B. Pharmacy course.
This book has been written as per the syllabus under the new education regulations (6, 7 & 8 of the Bachelor of Pharmacy (B. Pharm) course regulations 2014) by Pharmacy Council of India, New Delhi.
Analytical chemistry is an experimental Science. Chemistry laboratory aids the students in the study of science by clearly illustrating the principles and steps involved. The primary objective is to give a detailed and systematic account of all the experiments. Matter is presented in simple, concise and understandable language so as to make laboratory work as methodical and efficient as possible. The salient features of the book are:
• Manual contains 19 experiments as per the syllabus prescribed by Pharmacy Council of India.
• Experiment format provides clear instructions and Calculations.
• Simple and stepwise description of the experimental procedure.
• Question bank at the end of the manual would be useful to the students to evaluate their understanding about the practical.
We hopefully believe that the book will be warmly received and would prove useful to the students. The best judges of the book are the concerned subject teachers and the students for whom it is written. Comments and suggestions for further improvement of the book are always welcome.
- Authors
Acknowledgements
I owe my sincere thanks to Ms Bharti Mangla, Research Scholar, Jamia Hamdard, New Delhi for providing useful assistance with the writing and correction of the second edition of this book.
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